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Beilstein J. Org. Chem. 2015, 11, 897–905, doi:10.3762/bjoc.11.101
Graphical Abstract
Figure 1: Structures of some marine natural products 1–4.
Figure 2: Structures 5–7.
Scheme 1: Intramolecular gold(I)-catalyzed cyclization reaction of 8 to give 9 and 10.
Scheme 2: Synthesis of 13 and its reaction with AuCl3.
Scheme 3: Synthesis of 6.
Figure 3: Geometry optimized structures of 6, 7, 30 and 31.
Scheme 4: Reaction of 15 with Au(I)/AgOTf in the presence of EtOH and CD3OD.
Scheme 5: Reaction of 7 with Au(I)/AgOTf in the presence of EtOH.
Scheme 6: Proposed reaction mechanism for the intramolecular gold-catalyzed cyclization followed by EtOH addi...